C12/C13-ratio determination in nanodiamonds by atom-probe tomography

Autor: Josiah B, Lewis, Dieter, Isheim, Christine, Floss, David N, Seidman
Rok vydání: 2014
Zdroj: Ultramicroscopy.
ISSN: 1879-2723
Popis: The astrophysical origins of ∼ 3 nm-diameter meteoritic nanodiamonds can be inferred from the ratio of C12/C13. It is essential to achieve high spatial and mass resolving power and minimize all sources of signal loss in order to obtain statistically significant measurements. We conducted atom-probe tomography on meteoritic nanodiamonds embedded between layers of Pt. We describe sample preparation, atom-probe tomography analysis, 3D reconstruction, and bias correction. We present new data from meteoritic nanodiamonds and terrestrial standards and discuss methods to correct isotopic measurements made with the atom-probe tomograph.
Databáze: OpenAIRE