| Autor: |
V P, Shevchenko, I Iu, Nagaev, I S, Levina, L E, Kulikova, N F, Miasoedov, A V, Kamernitzkiĭ |
| Rok vydání: |
2010 |
| Předmět: |
|
| Zdroj: |
Bioorganicheskaia khimiia. 36(2) |
| ISSN: |
0132-3423 |
| Popis: |
1,2-Tritium-labeled 3-(O-carboxypropyl)- and 3-(O-carbomethoxypropyl)-oximes of 6alpha-methyl-16alpha,17alpha-cyclohexanopregn-4-ene-3,20-diones were obtained by the homogeneous catalytic hydrogenation of 1,2-dehydroprecursors with gaseous tritium and the subsequent separation of the resulting mixtures by HPLC. The specific radioactivities of 50-55 Ci/mmol were prepared using tris-(triphenylphosphine)-rhodium chloride. |
| Databáze: |
OpenAIRE |
| Externí odkaz: |
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