Coprecipitation-assisted coacervative extraction coupled to high-performance liquid chromatography: An approach for determining organophosphorus pesticides in water samples

Autor: Sabrina B, Mammana, Paula, Berton, Alejandra B, Camargo, Gustavo E, Lascalea, Jorgelina C, Altamirano
Rok vydání: 2016
Předmět:
Zdroj: Electrophoresis. 38(9-10)
ISSN: 1522-2683
Popis: An analytical methodology based on coprecipitation-assisted coacervative extraction coupled to HPLC-UV was developed for determination of five organophosphorus pesticides (OPPs), including fenitrothion, guthion, parathion, methidathion, and chlorpyrifos, in water samples. It involves a green technique leading to an efficient and simple analytical methodology suitable for high-throughput analysis. Relevant physicochemical variables were studied and optimized on the analytical response of each OPP. Under optimized conditions, the resulting methodology was as follows: an aliquot of 9 mL of water sample was placed into a centrifuge tube and 0.5 mL sodium citrate 0.1 M, pH 4; 0.08 mL Al
Databáze: OpenAIRE