[Determination of microelements from different types of grass in the habitat of Przewalski's gazelle by sealed microwave digestion ICP-AES]

Autor: Li-ye, Zhou, Guo-sheng, Xin, Xiu-ying, Pu
Rok vydání: 2012
Předmět:
Zdroj: Guang pu xue yu guang pu fen xi = Guang pu. 32(4)
ISSN: 1000-0593
Popis: For the mixture forge from different types of grassland, trace elements including copper, manganese, iron, zinc and molybdenum were separately determined by ICP-AES using high pressure system-sealed microwave digestion in the habitat of the Przewalski's gazelle in Qinghai Hudong in summer (mid-June), autumn (mid-September) and winter (mid-December). The samples of mixture forage were digested with HNO3-H2O2 acids system. The detection limits of the method for the elements varied from 0.002 to 0.008 microg x g(-1), with relative standard deviations between 0.13% and 4.29%, and the spike recovery ratios for them were in the range from 94.0% to 101.30%. This method was simple, sensitive and precise compared with conventional method, which will provide scientific basis for the research on gazelles habitat condition.
Databáze: OpenAIRE