| Autor: |
V K, Shormanov, Iu N, Baranov, E P, Duritsyn, S V, Maslov, E I, Pronichenko, S V, Ganiev |
| Rok vydání: |
2011 |
| Předmět: |
|
| Zdroj: |
Sudebno-meditsinskaia ekspertiza. 53(6) |
| ISSN: |
0039-4521 |
| Popis: |
Optimal conditions for the extraction of bancol from the biological material with toluene are described. The possibility of its purification and separation from co-extracted compounds on a silicagel L column, 40/100 mcm is illustrated. Identification and quantitative determination of bancol isolated from the cadaverous liver were performed by the electron spectrophotometry technique, thin-layer chromatography, and high performance liquid chromatography using normal-phase sorbents. A method of bancol detection was adapted for the purpose of forensic medical expertise and applied for the postmortem examination of the cadaverous tissues. |
| Databáze: |
OpenAIRE |
| Externí odkaz: |
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