Enantiomeric resolution by HPLC of axial chiral amides using amylose tris[(S)-1-phenylethylcarbamate]

Autor:	Q B, Cass, A L, Degani, M E, Tiritan, S A, Matlin, D P, Curran, A, Balog
Rok vydání:	1997
Předmět:	Spectrophotometry Ultraviolet Stereoisomerism Amylose Ion Exchange Resins Particle Size Cellulose Amides Chromatography High Pressure Liquid
Zdroj:	Chirality. 9(2)
ISSN:	0899-0042
Popis:	The enantiomeric resolution of a series of N-arylamides was examined on amylose tris[(S)-1-phenylethylcarbamate] coated onto aminopropylated 7 microns silica with 500 A diameter pores and on naked silica 5 microns particle size with 500 A diameter pores. The enantiomeric resolution obtained for this series was excellent on both columns. The enantioselectivity of cellulose and amylose tris(3,5-dimethylphenylcarbamate) coated onto APS-Hypersil (120 A pore size, 5 microns particle size) was also investigated for this series of compounds.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=pmid________::08b5706fcd8818c4675969e3d1e0f75b https://pubmed.ncbi.nlm.nih.gov/9134693 Zobrazit plný text záznamu Plný text