Annealed nanopowder GdVO4 :Sm3+ prepared by solution combustion synthesis

Autor: Rabasović, Maja, Šević, Dragutin, Križan, Janez, Rabasović, M. D., Savić-Šević, S., Mitrić, Miodrag, Petrović, M., Gilić, M., Romčević, Nebojša Ž.
Jazyk: angličtina
Rok vydání: 2017
Zdroj: Advanced Ceramics and Application : 5th Serbian Ceramic Society Conference : program and the book of abstracts; September 21-23, 2016; Belgrade
Popis: The gadolinium vanadate doped with samarium (GdVO4 :Sm3+) nanopowder was prepared by the solution combustion synthesis (SCS) method. After synthesis, in order to achieve the full crystallinity, the material was annealed in air atmosphere at 1300 °C. Phase identification in the post-annealed powder samples were performed by X-ray diffraction, and morphology was investigated by high resolution scanning electron microscope (SEM). Photoluminescence characterization including excitation and emission spectra and lifetime analysis has been done using tunable laser optical parametric oscillator excitation and streak camera. Several strong emission bands in Sm3+ emission spectrum were observed, located at 563 nm (4 G5/2 – 6 H5/2), 600 nm (4 G5/2 – 6 H7/2,), and 644 (653) nm (4 G5/2 – 6 H9/2,), respectively. The weak emission at 700-710 nm (4 G5/2 – 6 H11/2) was also observed by detection system. V Serbian Ceramic Society Conference - Advanced Ceramics and Application : new frontiers in multifunctional material science and processing : program and the book of abstracts; September 21-23, 2016; Belgrade
Databáze: OpenAIRE