Coordination compounds of zinc acetates with pyridinecarboxamides
| Autor: | Radić, Tanja |
|---|---|
| Přispěvatelé: | Kristl, Matjaž |
| Jazyk: | slovinština |
| Rok vydání: | 2013 |
| Předmět: |
Thermogravimetric analysis (TGA)
Fourier transform infrared spectroscopy (FTIR) rentgenska praškovna difrakcija (RPD) Zinc(II) acetate dihydrate koordinacijske spojine Pyridinecarboxamides X-ray powder diffraction (XRD) izonikotinamid Fourierjeva transformacijska infrardeča spektroskopija (FTIR) piridinkarboksamidi (nikotinamid pikolinamid) Coordination compounds udc:54(043.2) Cinkov(II) acetat dihidrat termogravimetrična analiza (TGA) |
| Zdroj: | Maribor |
| Popis: | Namen diplomske naloge je bil sinteza novih cinkovih koordinacijskih spojin iz cinkovega(II) acetata dihidrata in piridinkarboksamidov (izonikotinamid, nikotinamid in pikolinamid). Najprej smo sintetizirali cinkov(II) hidroksid, ki smo ga potem uporabili za sintezo cinkovega(II) acetata dihidrata. Izvajali smo reakcije med cinkovim(II) acetatom dihidratom in piridinkarboksamidi. Sintetizirane kristale smo karakterizirali z rentgensko praškovno difrakcijo, termogravimetrično analizo in Fourierjevo transformacijsko infrardečo spektroskopijo. Moje delo je bilo namenjeno sintezi in karakterizaciji novih koordinacijskih spojin. The purpose of this diploma work was to synthesize new zinc coordination compounds out of zinc(II) acetate dihydrate and pyridinecarboxamides (isonicotinamide, nicotinamide and picolinamide). First we synthesized zinc(II) hydroxide, which was further on used to synthesize zinc(II) acetate dihydrate. We carried out the reaction between zinc(II) acetate dihydrate and pyridinecarboxamide. The synthesized crystals were characterised with X-ray powder diffraction (XRD), thermogravimetric analysis (TGA) and Fourier transform infrared spectroscopy (FTIR). My work was devoted to the synthesis and characterization of new coordination compounds. |
| Databáze: | OpenAIRE |
| Externí odkaz: |
|