Investigation of structural, morphological and optical properties of nickel zinc oxide films prepared by sol–gel method
Autor: | Yasemin Caglar, D. Duygu Dogan, Mujdat Caglar, Saliha Ilican |
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Přispěvatelé: | Anadolu Üniversitesi, Fen Fakültesi, Fizik Bölümü, Çağlar, Yasemin, Ilıcan, Saliha, Çağlar, Müjdat |
Rok vydání: | 2011 |
Předmět: |
Spin coating
Materials science Mechanical Engineering Sol-Gel Process Metals and Alloys Analytical chemistry chemistry.chemical_element Crystal structure Crystalline Structure Crystallography Nickel Lattice constant chemistry Mechanics of Materials Absorption Edge Materials Chemistry Crystallite Nizno Wurtzite crystal structure Sol-gel Diffractometer |
Zdroj: | Journal of Alloys and Compounds. 509:2461-2465 |
ISSN: | 0925-8388 |
DOI: | 10.1016/j.jallcom.2010.11.054 |
Popis: | WOS: 000287167700209 NiZnO films have been prepared on glass substrates by sol-gel spin coating method. Nickel (II) nitrate hexahyrate and zinc acetate dihydrate were used as precursors. Surface morphology and crystalline structure of the films were investigated by field emission scanning electron microscopy (FESEM) and X-ray diffractometer, respectively. X-ray diffraction (XRD) patterns showed that the films are polycrystalline nature. It was observed that crystal structure changed from wurtzite (ZnO) to cubic (NiO) structure. The lattice constants crystallite size and preferred orientation were calculated from XRD data. The surface morphology of the films changed with Ni concentration. The average transmittance of the ZnO film decreased from 84% to 58% in the visible region. The absorption edge varied from 3.26 to 3.89 eV with increasing Ni concentration Anadolu University Commission of Scientific Research [061039, 081029] This work was supported by Anadolu University Commission of Scientific Research Projects under grant no. 061039 and 081029. |
Databáze: | OpenAIRE |
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