Commercial yerba mate (Ilex paraguariensis) produced in South America: Determination of dithiocarbamate residues by gas chromatography-mass spectrometry

Autor: Rosselei Caiel da Silva, Ingrid Duarte dos Santos, Júlia Paula Neu, Robson Dias Wouters, Marlos Eduardo Zorzella Fontana, Priscila Dotto Rosa Balbinot, Roger Wagner, Ionara Regina Pizzutti
Rok vydání: 2021
Předmět:
Zdroj: Food chemistry. 394
ISSN: 1873-7072
Popis: This work presents an easy and quick miniaturized procedure for the analysis of dithiocarbamates fungicides (DTC), by GC-MS, in yerba mate, an important product in South America. The sample amount, the volume of extracting solvent and acid solution, and the time of hot bath shaking were minimized. A clean-up procedure based on PSA, GCB and MgSO4 was studied in order to improve analytical signal and reduce GC-MS system damage. Blank yerba mate samples were spiked with thiram at equivalent CS
Databáze: OpenAIRE