Heat source and voiding signatures of Mullins damage in filled EPDM

Autor: Jean-Luc Bouvard, Guillaume Corvec, Noëlle Billon, Oguzhan Oguz, Christophe Pradille, Edith Peuvrel-Disdier, Nicolas Candau, Maria Lluisa Maspoch
Přispěvatelé: Centre Català del Plàstic (CCP), Universitat Politècnica de Catalunya Barcelona Tech (EEBE-UPC), Ecole Polytech Fed Lausanne, EPFL STI IMX LMOM, Inst Mat, Lab Macromol & Organ Mat,Stn 12, CH-1015 Lausanne, Switzerland, Centre de Mise en Forme des Matériaux (CEMEF), MINES ParisTech - École nationale supérieure des mines de Paris, Université Paris sciences et lettres (PSL)-Université Paris sciences et lettres (PSL)-Centre National de la Recherche Scientifique (CNRS), Mat Xper, Universitat Politècnica de Catalunya. Departament de Ciència i Enginyeria de Materials, Universitat Politècnica de Catalunya. e-PLASCOM - Plàstics i Compòsits Ecològics
Jazyk: angličtina
Rok vydání: 2020
Předmět:
Digital image correlation
mechanical-behavior
Materials science
Polymers and Plastics
Polymers
Nucleation
strain-induced crystallization
02 engineering and technology
010402 general chemistry
Enginyeria dels materials [Àrees temàtiques de la UPC]
01 natural sciences
composites
Natural rubber
[SPI.MECA.MEMA]Engineering Sciences [physics]/Mechanics [physics.med-ph]/Mechanics of materials [physics.class-ph]
Rubber damage
Composite material
rubber damage
Softening
ComputingMilieux_MISCELLANEOUS
density
natural rubbers
Strain (chemistry)
Organic Chemistry
self-heating
deformation
temperature
dependence
021001 nanoscience & nanotechnology
0104 chemical sciences
Polímers
Filled EPDM
Self-heating
kinetics
visual_art
Cavitation
Tangent modulus
filled epdm
visual_art.visual_art_medium
fatigue
Deformation (engineering)
0210 nano-technology
Zdroj: Polymer Testing
Polymer Testing, Elsevier, 2020, 91, pp.106838. ⟨10.1016/j.polymertesting.2020.106838⟩
UPCommons. Portal del coneixement obert de la UPC
Universitat Politècnica de Catalunya (UPC)
ISSN: 0142-9418
DOI: 10.1016/j.polymertesting.2020.106838⟩
Popis: The thermomechanical coupling of Mullins damage in filled EPDM has been investigated by analysing the self-heating via Infrared thermography (IR) and the voiding fraction by Digital Image Correlation (DIC). The volumetric strain measured during the rubber deformation is found to be predominantly associated with damage, while thermal dilatation caused by self-heating has a negligible contribution. On this basis, the thermomechanical coupling of Mullins phenomena has been identified by evaluating the strain and time dependence of the following criteria: the tangent modulus, the voiding rate and the heat sources. The tangent modulus that reaches a maximum at the strain transition from a series of cycle to another is found to be an appropriate mechanical signature of Mullin softening. At the same strain transition, both voiding rate upturn and heat source upturn are observed. These signatures suggest the Mullins damage to be mainly associated at high strain rate with the (re)-activation of dissipative cavitation mechanisms, by nucleation of new cavities and/or acceleration of cavities growth.
Databáze: OpenAIRE