Preparation of mesoporous ZrO2 with the middle phase formed in a trioctyl (or alkyl) phosphinic oxide-kerosene/HCl-ZrOCl2 extraction system
| Autor: | Lingling Yu, Xun Fu, Lei Chen, Linsheng Feng, Hai-tao Zhu, Jingyi Yang, Guohua Gu |
|---|---|
| Rok vydání: | 2003 |
| Předmět: |
chemistry.chemical_classification
Kerosene Materials science Precipitation (chemistry) Extraction (chemistry) Inorganic chemistry Oxide Surfaces Coatings and Films Electronic Optical and Magnetic Materials Biomaterials Crystal chemistry.chemical_compound Colloid and Surface Chemistry chemistry Phase (matter) Mesoporous material Alkyl |
| Zdroj: | Journal of colloid and interface science. 265(1) |
| ISSN: | 0021-9797 |
| Popis: | The extraction behavior and phase behavior of TOPO (or TRPO)–kerosene/HCl–ZrOCl 2 systems have been investigated. The middle phase with bicontinuous structure is first used as both the Zr(IV) source and the template to prepare mesoporous material just by precipitation with aqua ammonia under low temperature. By this method, crystal mesoporous ZrO 2 powders with average d -values of 6.3 and 7.48 nm, respectively, have been obtained. TG-DTA, TEM, and XRD are adopted for the characterization of the synthesized sample. |
| Databáze: | OpenAIRE |
| Externí odkaz: |
|
Full Text from ScienceDirect