Interlaboratory study on rheological properties of cement pastes and reference substances: comparability of measurements performed with different rheometers and measurement geometries

Autor: Joachim Jürgen Riedmiller, Mareike Thiedeitz, Shirin Fataei, Hans-W. Krauss, Tabea von Bronk, Manfred Wilhelm, Inga Hauschildt, Steffen Jesinghausen, Irina Ivanova, Viktor Mechtcherine, Sebastian Pawelczyk, Dietmar Stephan, Christian Baumert, O. Mazanec, Christoph Gehlen, Christopher O. Klein, Sarah Leinitz, Egor Secrieru, Dario Cotardo, Ludger Lohaus, Michael Haist, Nonkululeko W. Radebe, Hans-Joachim Schmid, Dirk Lowke, Ursula Pott, Wolfram Schmidt, Mahmoud Eslami Pirharati, Julian Link, David Nicia, Harald Garrecht
Rok vydání: 2020
Předmět:
plastic viscosity
geometry
Materials science
ultrasonics
Rheometer
rheological property
0211 other engineering and technologies
02 engineering and technology
rheological measurements
Cement paste
reference substance
interlaboratory studies
Plastic viscosity
reproducibilities
Viscosity
ddc:690
Rheology
021105 building & construction
General Materials Science
Buildings
Composite material
rheometers
Civil and Structural Engineering
Cement
Reproducibility
Rheometry
Comparability
Building and Construction
measurement geometry
021001 nanoscience & nanotechnology
cements
ddc
yield stress
Interlaboratory test
measurement setup
Mechanics of Materials
Test setup
Dewey Decimal Classification::600 | Technik::690 | Hausbau
Bauhandwerk

viscosity
rheology
Testing procedure
Ultrasound gel
0210 nano-technology
Zdroj: Materials and structures, 53 (4), Art. Nr.: 92
Materials and Structures 53 (2020), Nr. 4
ISSN: 1871-6873
1359-5997
0025-5432
DOI: 10.1617/s11527-020-01477-w
Popis: This paper presents the results of an interlaboratory study of the rheological properties of cement paste and ultrasound gel as reference substance. The goal was to quantify the comparability and reproducibility of measurements of the Bingham parameters yield stress and plastic viscosity when measured on one specific paste composition and one particular ultrasound gel in different laboratories using different rheometers and measurement geometries. The procedures for both in preparing the cement paste and carrying out the rheological measurements on cement paste and ultrasound gel were carefully defined for all of the study’s participants. Different conversion schemes for comparing the results obtained with the different measurement setups are presented here and critically discussed. The procedure proposed in this paper ensured a reasonable comparability of the results with a coefficient of variation for the yield stress of 27% and for the plastic viscosity of 24%, despite the individual measurement series’ having been performed in different labs with different rheometers and measurement geometries.
Deutsche Forschungsgemeinschaft
Projekt DEAL
Databáze: OpenAIRE