The Influence of pH Values on the Crystallite Size of ZnO by Solvothermal Synthesis

Autor:	Mochammad Zakki Fahmi, Ahmadi Jaya Permana, Hartati Hartati, Dian Wulandari, Harsasi Setyawati
Rok vydání:	2017
Předmět:	Inorganic Chemistry Solvothermal synthesis Materials science Chemical engineering chemistry Phase (matter) Semiconductor materials ZnO chemistry.chemical_element Crystallite Zinc Scherrer equation
Zdroj:	Jurnal Kimia Riset; Vol. 2 No. 2 (2017): Desember; 118-122
ISSN:	2528-0422 2528-0414
DOI:	10.20473/jkr.v2i2.6430
Popis:	Zinc oxide (ZnO) is a semiconductor material that widely used in various applications due to its unique properties. Synthesis of ZnO by solvothermal method has been conducted with controlled pH values. The variations of pH value were 10, 11 and 12 by adjusting NaOH content. Crystall structure of the synthesis products after heat treatment at 110oC and 600oC has characterised by X-ray Diffratometer (XRD). Crystallite size of ZnO was measured by Scherrer equation. Crystall phase of ZnO has been observed on all pH value variations at 110 oC with 22,98-37,06 nm of crystallite size, whereas ZnO has been observed on all pH value variations at 600 oC with 41,39-71,77 nm of crystallite size.Keywords: ZnO, pH values, crystallite size, solvothermal
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_dedup___::ef94905f62a620a245f84faaf2091a14 https://doi.org/10.20473/jkr.v2i2.6430 Zobrazit plný text záznamu