Oil extraction from enriched Spirulina platensis microalgae usingă supercritical carbon dioxide

Autor: Farid Chemat, Olivier Lépine, Maryline Abert Vian, Elisabeth Badens, Mohamed Zaier, Christelle Crampon, Clémence Nikitine, Celine Dejoye Tanzi
Přispěvatelé: Laboratoire de Mécanique, Modélisation et Procédés Propres (M2P2), Aix Marseille Université (AMU)-École Centrale de Marseille (ECM)-Centre National de la Recherche Scientifique (CNRS), Algosource, Sécurité et Qualité des Produits d'Origine Végétale (SQPOV), Institut National de la Recherche Agronomique (INRA)-Avignon Université (AU), Crampon, Christelle, Centre National de la Recherche Scientifique (CNRS)-École Centrale de Marseille (ECM)-Aix Marseille Université (AMU), Laboratoire de Génie des Procédés Catalytiques (LGPC), École Supérieure Chimie Physique Électronique de Lyon-Centre National de la Recherche Scientifique (CNRS)-Université Claude Bernard Lyon 1 (UCBL), Université de Lyon-Université de Lyon
Jazyk: angličtina
Rok vydání: 2017
Předmět:
0106 biological sciences
classe lipidique
General Chemical Engineering
Scale-up
Extraction
Laboratory scale
01 natural sciences
Autoclave
[SPI.MECA.MEFL]Engineering Sciences [physics]/Mechanics [physics.med-ph]/Fluids mechanics [physics.class-ph]
Supercritical CO2
Microalga
Neutral lipid
Antioxidant
RSM
antioxydant
010608 biotechnology
[SPI.GPROC]Engineering Sciences [physics]/Chemical and Process Engineering
Physical and Theoretical Chemistry
micro-algue
Spirulina (genus)
extraction au fluide supercritique
Chromatography
Supercritical carbon dioxide
acide gras
biology
010405 organic chemistry
Chemistry
Extraction (chemistry)
extraction d'huile
Condensed Matter Physics
biology.organism_classification
Supercritical fluid
0104 chemical sciences
Chemical engineering
spiruline
SCALE-UP
dioxyde de carbone supercritique
Zdroj: Journal of Supercritical Fluids
Journal of Supercritical Fluids, 2017, 119, pp.289-296. ⟨10.1016/j.supflu.2016.10.006⟩
Journal of Supercritical Fluids (119), 289-296. (2017)
Journal of Supercritical Fluids, Elsevier, 2017, 119, pp.289-296. ⟨10.1016/j.supflu.2016.10.006⟩
ISSN: 0896-8446
DOI: 10.1016/j.supflu.2016.10.006⟩
Popis: International audience; This article deals with the extraction of neutral lipids andă antioxidants from enriched Spirulina platensis microalgae usingă supercritical carbon dioxide (CO2), and more particularly with theă influence of experimental conditions on extraction yields and kineticsă at laboratory and pilot scales. Preliminary studies were carried out ată laboratory scale before the establishment of an experimental design:ă extraction curves were plotted for different autoclave fill rates, andă under different conditions of pressure and temperature. Using a Responseă Surface Methodology, the significant influence of pressure on extractionă efficiency was highlighted. Surface responses showed that, in theă studied experimental field, mass loss increased when pressure,ă temperature, and CO2/microalgae mass ratio increased. Extract analysesă showed that oil extracts contained chlorophylls a and b, as well asă beta-carotene. Finally, larger-scale experiments were carried out withă batches of 1 and 50 kg (scale-factors of 100 and 5000, respectively) andă the results were consistent with those obtained at laboratory scale. (C)ă 2016 Elsevier B.V. All rights reserved.
Databáze: OpenAIRE