Synthesis of Highly Functionalized N , N ‐Diarylamides by an Anodic C, N ‐Coupling Reaction

Autor:	Siegfried R. Waldvogel, Robert Franke, Sebastian Lips, Maurice Dörr, Carlos A. Martínez-Huitle, Dieter Schollmeyer
Rok vydání:	2019
Předmět:	Green chemistry 010405 organic chemistry Chemistry Organic Chemistry General Chemistry Electrolyte 010402 general chemistry Electrosynthesis Electrochemistry 01 natural sciences Combinatorial chemistry Catalysis Coupling reaction 0104 chemical sciences Anode Constant current
Zdroj:	Chemistry – A European Journal. 25:7835-7838
ISSN:	1521-3765 0947-6539
DOI:	10.1002/chem.201901442
Popis:	We report an innovative, sustainable and straightforward protocol for the synthesis of N,N-diarylamides equipped with nonprotected hydroxyl groups by using electrosynthesis. The concept allows the application of various substrates furnishing diarylamides with yields up to 57 % within a single and direct electrolytic protocol. The method is thereby easy to conduct in an undivided cell with constant current conditions offering a versatile and short-cut alternative to conventional pathways.
Databáze:	OpenAIRE
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