Development of decahydronaphthalene reference material for low flash point measurements
| Autor: | S. Zakel, Ibrahim F. Tahoun, Harby E. Ahmed |
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| Rok vydání: | 2021 |
| Předmět: |
Value assignment
020209 energy Flash point 02 engineering and technology Certification Catalysis 020401 chemical engineering Geochemistry and Petrology 0202 electrical engineering electronic engineering information engineering 0204 chemical engineering Process engineering lcsh:Petroleum refining. Petroleum products Renewable Energy Sustainability and the Environment business.industry Process Chemistry and Technology Organic Chemistry Testing equipment Metrology Fuel Technology Certified reference materials lcsh:TP690-692.5 Environmental science Measurement uncertainty Reference material business |
| Zdroj: | Egyptian Journal of Petroleum, Vol 30, Iss 1, Pp 7-10 (2021) |
| ISSN: | 1110-0621 |
| DOI: | 10.1016/j.ejpe.2020.12.002 |
| Popis: | Certified reference materials are an essential tool for calibration of testing equipment, validation of analytical methods and ensuring quality of test results. Due to lack of national low temperature reference materials, Decahydronaphthalene reference material for flash point measurements according to ISO 13736has been developed by the National Metrology Institute of Egypt (NIS). This article describes production steps of the reference material. Certification of the material was carried out by interlaboratory comparisons, where between bottles homogeneity and stability studies were conducted in explosion protection department at PTB, Germany. The interlaboratory results were statistically analyzed, and robust mean was calculated as assigned value. The certified value and expanded measurement uncertainty (k = 2) was found 55.7 °C ± 1.2 °C, respectively. |
| Databáze: | OpenAIRE |
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