High-Performance Liquid Chromatography evaluation of phenols in olive fruit, virgin olive oil, vegetation waters, and pomace and 1D- and 2D-Nuclear Magnetic Resonance characterization
Autor: | Enrico Miniati, Alceo Macchioni, Gianfrancesco Montedoro, Maurizio Servili, Maura Baldioli, Roberto Selvaggini |
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Jazyk: | angličtina |
Rok vydání: | 1999 |
Předmět: |
Chromatography
biology General Chemical Engineering Organic Chemistry Extraction (chemistry) Pomace biology.organism_classification High-performance liquid chromatography chemistry.chemical_compound Nuclear magnetic resonance chemistry Oleuropein Oleaceae Phenols Solid phase extraction Elenolic acid |
Zdroj: | Scopus-Elsevier |
Popis: | Phenolic compounds are the most important antioxidants of virgin olive oil. This paper reports on the application of solid phase extraction (SPE) in the separation of phenolic compounds from olive fruit, olive oil, and by-products of the mechanical extraction of the oil and the complete spectroscopic characterization by nuclear magnetic resonance of demethyloleuropein and verbascoside extracted from olive fruit. SPE led to a higher recovery of phenolic compounds from olives than did liquid/liquid extraction. SPE also was used to separate phenolic compounds from pomaces and vegetation waters. Phenylacid and phenyl-alcohol concentrations in extracts obtained from SPE and liquid/liquid extraction were not significantly different (P |
Databáze: | OpenAIRE |
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