Multiresidue method for triazines and pyrethroids determination by solid-phase extraction and gas chromatography-tandem mass spectrometry
| Autor: | Raquel A L Ribeiro, Daniela R. Lachter, Angela de Luca Rebello Wagener, Carlos German Masone, Adriana Haddad Nudi, Giovana F Porto |
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| Rok vydání: | 2020 |
| Předmět: |
Crops
Agricultural Food Contamination 010501 environmental sciences Quechers Fragaria 01 natural sciences Gas Chromatography-Mass Spectrometry Solanum lycopersicum Tandem Mass Spectrometry Pyrethrins Solid phase extraction 0105 earth and related environmental sciences Mangifera Chromatography Gas Chromatography/Tandem Mass Spectrometry Pesticide residue Triazines Chemistry Solid Phase Extraction 010401 analytical chemistry Pesticide Residues General Medicine Pesticide Pollution 0104 chemical sciences Malus Extraction methods Cucumis sativus Brazil Food Science |
| Zdroj: | Journal of Environmental Science and Health, Part B. 55:865-875 |
| ISSN: | 1532-4109 0360-1234 |
| DOI: | 10.1080/03601234.2020.1790266 |
| Popis: | This research aimed at implementing and validating a method for analysis of pesticide residues in crops. QuEChERS extraction method with PSA purification was used following analyzes by gas chromatography with tandem mass spectrometry in Selected Reaction Monitoring mode. A short run method was successfully developed for the determination of 41 pesticides, confirmed by two precursor-products for each analyte. The calibration curve for each analyte was linear at concentration range from 1 to 500 μg kg |
| Databáze: | OpenAIRE |
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