Structure investigation on a novel 2-halo-2,3-unsaturated-N-galactoside, NMR and X-ray diffraction of a monoclinic multidomain crystal
| Autor: | Leticia Lafuente, Oscar E. Piro, Gustavo A. Echeverría, Agustín H. Rojas, Agustín Ponzinibbio, Virginia Vetere |
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| Rok vydání: | 2021 |
| Předmět: |
Diffraction
Models Molecular Magnetic Resonance Spectroscopy Chemistry Organic Chemistry Galactosides General Medicine Crystallography X-Ray Biochemistry Galactoside Analytical Chemistry Crystal Crystallography chemistry.chemical_compound X-ray crystallography Carbohydrate Conformation Halo Single crystal Derivative (chemistry) Monoclinic crystal system |
| Zdroj: | Carbohydrate research. 510 |
| ISSN: | 1873-426X |
| Popis: | Single crystal X-ray and NMR investigations on multidomain structured N-(4,6-di-O-acetyl-2,3-dideoxy-α-D-threo-hex-2-en-2-iodo-pyranosyl)-methylsulfonamide are reported. This is the first crystallographic diffraction data report related to a 2-halo-2,3-unsaturated galactoside derivative. A complete structural study, including conformations and crystal packing, was performed by analyzing the spectroscopic data in solid state (XRD) and in solution (NMR). |
| Databáze: | OpenAIRE |
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