Interpenetrated Magnesium–Tricalcium Phosphate Composite: Manufacture, Characterization and In Vitro Degradation Test
| Autor: | Lenka Klakurková, Mariano Casas-Luna, Sebastian Diaz-de-la-Torre, Pavel Gejdoš, Ladislav Čelko, Miroslava Horynová, Edgar B. Montufar, Serhii Tkachenko, Jozef Kaiser |
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| Jazyk: | angličtina |
| Rok vydání: | 2017 |
| Předmět: |
Materials science
Scanning electron microscope 0206 medical engineering Composite number chemistry.chemical_element Spark plasma sintering SPS 02 engineering and technology Industrial and Manufacturing Engineering chemistry.chemical_compound Magnesium Porosity Bone regeneration kalcium fosfát Metallurgy Metals and Alloys horčík koroze Liquid metal infiltration 021001 nanoscience & nanotechnology Phosphate Microstructure 020601 biomedical engineering infiltrace tekutým kovem Corrosion chemistry Chemical engineering Calcium phosphate 0210 nano-technology |
| Zdroj: | Acta Metallurgica Sinica (English Letters). 2017, vol. 30, issue 4, p. 319-325. Acta Metallurgica Sinica (English Letters) |
| Popis: | Magnesium and calcium phosphates composites are promising biomaterials to create biodegradable load-bearing implants for bone regeneration. The present investigation is focused on the design of an interpenetrated magnesium–tricalcium phosphate (Mg–TCP) composite and its evaluation under immersion test. In the study, TCP porous preforms were fabricated by robocasting to have a prefect control of porosity and pore size and later infiltrated with pure commercial Mg through current-assisted metal infiltration (CAMI) technique. The microstructure, composition, distribution of phases and degradation of the composite under physiological simulated conditions were analysed by scanning electron microscopy, elemental chemical analysis and X-ray diffraction. The results revealed that robocast TCP preforms were full infiltrated by magnesium through CAMI, even small pores below 2 lm have been filled with Mg, giving to the composite a good interpenetration. The degradation rate of the Mg–TCP composite displays lower value compared to the one of pure Mg during the first 24 h of immersion test. Magnesium and calcium phosphates composites are promising biomaterials to create biodegradable load-bearing implants for bone regeneration. The present investigation is focused on the design of an interpenetrated magnesium–tricalcium phosphate (Mg–TCP) composite and its evaluation under immersion test. In the study, TCP porous preforms were fabricated by robocasting to have a prefect control of porosity and pore size and later infiltrated with pure commercial Mg through current-assisted metal infiltration (CAMI) technique. The microstructure, composition, distribution of phases and degradation of the composite under physiological simulated conditions were analysed by scanning electron microscopy, elemental chemical analysis and X-ray diffraction. The results revealed that robocast TCP preforms were full infiltrated by magnesium through CAMI, even small pores below 2 lm have been filled with Mg, giving to the composite a good interpenetration. The degradation rate of the Mg–TCP composite displays lower value compared to the one of pure Mg during the first 24 h of immersion test. |
| Databáze: | OpenAIRE |
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