Analysis of acetamiprid in vegetables using gas chromatography-tandem mass spectrometry
| Autor: | F. Javier Arrebola, José Luis Martínez Vidal, Manuel Mateu-Sánchez, Mercedes Moreno |
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| Rok vydání: | 2003 |
| Předmět: |
Chromatography
Gas Chromatography/Tandem Mass Spectrometry Pyridines Extraction (chemistry) Ethyl acetate Reproducibility of Results Tandem mass spectrometry Mass spectrometry Acetamiprid Gas Chromatography-Mass Spectrometry Analytical Chemistry chemistry.chemical_compound Neonicotinoids chemistry Vegetables Gas chromatography Quantitative analysis (chemistry) |
| Zdroj: | Analytical sciences : the international journal of the Japan Society for Analytical Chemistry. 19(5) |
| ISSN: | 0910-6340 |
| Popis: | A new analytical method has been validated for determining the insecticide acetamiprid in vegetables using gas chromatography (OC) and different mass spectrometric detection techniques, such as full-scan mass spectrometry (MS), and tandem mass spectrometry (MS/MS). For this purpose, a previous extraction of the vegetable sample was carried out with ethyl acetate. In GC-MS/MS, the lowest detectable concentration was 0.001 mg kg(-1), the average recovery rates at various fortification levels (0.015 and 0.030 mg kg(-1)) ranged between 82.4 and 85.7% and the relative standard deviations were lower than 12.2% in all cases. |
| Databáze: | OpenAIRE |
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