Metal-free synthesis of 2-mercaptobenzothiazoles and 6-(4-substituted-1H-1,2,3-triazol-1-yl)-2-mercaptobenzothiazoles via microwave-assisted synthesis pathway

Autor: Truong Thanh Tung, Luong Xuan Huy
Rok vydání: 2020
Předmět:
Zdroj: Synthetic Communications. 50:2007-2014
ISSN: 1532-2432
0039-7911
DOI: 10.1080/00397911.2020.1761984
Popis: A simple, efficient, and metal-free methodology for the preparation of 2-mercaptobenzothiazole and derivatives in excellent yields via microwave-assisted pathway is reported. Our condition provides a convenient protocol for the synthesis of a diverse collection of 2-mercaptobenzothiazoles and 6-(4-substituted-1H-1,2,3-triazol-1-yl)-2-mercaptobenzothiazoles with a very simple purification process. This report provides an alternative protocol for fast access to the wide range of compounds for sequence synthesis and biological studies.
Databáze: OpenAIRE
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