| Popis: |
Separation of free fatty acids and triglycerides is important in the edible oil industry. In this study, both experimental and simulation approaches were conducted using falling film molecular distillation. A binary mixture of oleic acid as free fatty acid with refined soybean oil as triglyceride was used. Evaporation temperature range tested was from 110 to 160 °C, while other parameters such as condensation temperature, feeding rate, and vacuum pressure were fixed. The free fatty acid content of retentate was gradually decreased as evaporation temperature increased, while the free fatty acid content of distillate was approximately 100 wt.%, regardless of temperature. Triglycerides had an extremely low vapor pressure compared to oleic acid; therefore, their fraction in distillate was negligible. The mass conservation and transport equations were selected to explain the evaporation mechanism, and analytical solutions were simply introduced under the conditions of low mass fraction of volatile compound in the feeding mixture. Some experimental data are re-quired to determine the coefficient of molecular distillation in the governing equation. Using this obtained parameter, the proposed model could simulate all mass amounts and fractions of each component in retentate and distillate with a good agreement between experimental and simulation data, indicating the reasonable accuracy of the model proposed. |
