Size characterization of airborne SiO2 nanoparticles with on-line and off-line measurement techniques: an interlaboratory comparison study
| Autor: | Sebastien Ducourtieux, Sylvain Bondiguel, Loukie Adlem, François Gensdarmes, François Gaie-Levrel, C.S. Kim, Graham R. Johnson, Thor E. Bostrom, Lidia Morawska, A. Salas, Vasile-Dan Hodoroaba, Young Heon Kim, Camilla Costa, Keiji Takahata, Kai Dirscherl, J.A. Guardado, T. Macé, C. Motzkus, Alexandra Delvallée, Åsa K. Jämting, Patrick Ausset, O. Popov, M.C. Chu, Ehsan Majd Faghihi, Ilya Kuselman, Inna Popov, S. Vaslin-Reimann, Gustavo Capannelli, Kensei Ehara, M. Maille, Malcolm Lawn, N. Michielsen |
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| Přispěvatelé: | National Metrology Institute of South Africa, Laboratoire National de Métrologie et d’Essais (LNE), Danish Institute of Fundamental Metrology, BAM Federal Institute for Materials Research and Testing, Federal Institute for Materials Research and Testing - Bundesanstalt für Materialforschung und -prüfung (BAM), The Hebrew University of Jerusalem (HUJ), National Metrology Institute of Japan, National Institute od Advanced Industrial Science and Technology, Laboratoire Interuniversitaire des Systèmes Atmosphériques (LISA (UMR_7583)), Institut national des sciences de l'Univers (INSU - CNRS)-Université Paris-Est Créteil Val-de-Marne - Paris 12 (UPEC UP12)-Centre National de la Recherche Scientifique (CNRS)-Université Paris Cité (UPCité), Laboratoire de Physique et de Métrologie des Aérosols (IRSN/DSU/SERAC/LPMA), Institut de Radioprotection et de Sûreté Nucléaire (IRSN), International Laboratory for Air Quality and Health [Brisbane], Queensland University of Technology [Brisbane] (QUT), Korea Research Institute of Standards and Science [Daejon] (KRISS), KRISS, Department of Chemistry and Industrial Chemistry, Genova University, Università degli studi di Genova = University of Genoa (UniGe), Institut national des sciences de l'Univers (INSU - CNRS)-Université Paris-Est Créteil Val-de-Marne - Paris 12 (UPEC UP12)-Centre National de la Recherche Scientifique (CNRS)-Université de Paris (UP), Laboratoire de Physique et de Métrologie des Aérosols (DSU/SERAC/LPMA), Universita degli studi di Genova |
| Rok vydání: | 2013 |
| Předmět: |
010504 meteorology & atmospheric sciences
aerosol Analytical chemistry Nanoparticle 02 engineering and technology 01 natural sciences Characterization measurement Atomic force microscopy Mica electrostatic precipitation General Materials Science [PHYS]Physics [physics] silicon dioxide education.field_of_study Electrostatic separators evaluation Spectrometers nanoparticle article Particle size 021001 nanoscience & nanotechnology Condensed Matter Physics Atomic and Molecular Physics and Optics unclassified drug Metrology Characterization (materials science) Interlaboratory comparison studies priority journal Modeling and Simulation Uncertainty analysis Measurement uncertainty Nanoparticles characterizations 0210 nano-technology Scanning mobility Scanning electron microscopy Scanning and transmission electron microscopy Materials science Characterization Population Bioengineering Shape memory effect Interlaboratory comparison transmission electron microscopy Calibration controlled study education 0105 earth and related environmental sciences Aerosols Spectrometer silicon dioxide nanoparticle Size distribution General Chemistry calibration scanning mobility particle size spectrometer Nanoparticles measurement spectrometer Metrological traceabilitys |
| Zdroj: | Journal of Nanoparticle Research Journal of Nanoparticle Research, 2013, 15 (10), ⟨10.1007/s11051-013-1919-4⟩ |
| ISSN: | 1572-896X 1388-0764 |
| DOI: | 10.1007/s11051-013-1919-4 |
| Popis: | Results of an interlaboratory comparison on size characterization of SiO2 airborne nanoparticles using on-line and off-line measurement techniques are discussed. This study was performed in the framework of Technical Working Area (TWA) 34 - "Properties of Nanoparticle Populations" of the Versailles Project on Advanced Materials and Standards (VAMAS) in the project no. 3 "Techniques for characterizing size distribution of airborne nanoparticles". Two types of nano-aerosols, consisting of (1) one population of nanoparticles with a mean diameter between 30.3 and 39.0 nm and (2) two populations of non-agglomerated nanoparticles with mean diameters between, respectively, 36.2-46.6 nm and 80.2-89.8 nm, were generated for characterization measurements. Scanning mobility particle size spectrometers (SMPS) were used for on-line measurements of size distributions of the produced nano-aerosols. Transmission electron microscopy, scanning electron microscopy, and atomic force microscopy were used as off-line measurement techniques for nanoparticles characterization. Samples were deposited on appropriate supports such as grids, filters, and mica plates by electrostatic precipitation and a filtration technique using SMPS controlled generation upstream. The results of the main size distribution parameters (mean and mode diameters), obtained from several laboratories, were compared based on metrological approaches including metrological traceability, calibration, and evaluation of the measurement uncertainty. Internationally harmonized measurement procedures for airborne SiO2 nanoparticles characterization are proposed. © 2013 Springer Science+Business Media Dordrecht. |
| Databáze: | OpenAIRE |
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