Identification of urinarym-hydroxyphenylhydracrylic acid by gas chromatography-mass spectrometry
Autor: | J. H. Duncan, Katherine N Scott, G. Gotthelf, Margaret W. Couch |
---|---|
Rok vydání: | 1974 |
Předmět: |
Chromatography
Gas Magnetic Resonance Spectroscopy Chromatography Phenylpropionates Trimethylsilyl Ether Mass spectrometry Methylation Biochemistry Mass Spectrometry chemistry.chemical_compound Acrylates chemistry Cinnamates Proton NMR Humans Molecular Medicine Gas chromatography Gas chromatography–mass spectrometry Spectroscopy Derivative (chemistry) |
Zdroj: | Biological Mass Spectrometry. 1:40-42 |
ISSN: | 1096-9888 1052-9306 |
DOI: | 10.1002/bms.1200010109 |
Popis: | β-(m-Hydroxyphenyl)hydracrylic acid has been identified in human urine by gas chromatography, high and low reso ution mass spectrometry, and proton nuclear magnetic resonance spectroscopy. A rapid and conclusive method is presented for the identification of this acid as its methyl ester and/or its methyl ester trimethylsilyl ether derivative by combined gas chromatography-mass spectrometry. |
Databáze: | OpenAIRE |
Externí odkaz: |