Early commissioning results for spectroscopic X-ray Nano-Imaging Beamline BL 7C sXNI at PLS-II

Autor: Sangsul Lee, Jun Lim, Ik-Hwan Kwon, Sechang Kang, Jae Young Kim, Sung Sun Yang
Rok vydání: 2017
Předmět:
Zdroj: Journal of Synchrotron Radiation. 24:1276-1282
ISSN: 1600-5775
Popis: For spectral imaging of chemical distributions using X-ray absorption near-edge structure (XANES) spectra, a modified double-crystal monochromator, a focusing plane mirrors system and a newly developed fluorescence-type X-ray beam-position monitoring and feedback system have been implemented. This major hardware upgrade provides a sufficiently stable X-ray source during energy scanning of more than hundreds of eV for acquisition of reliable XANES spectra in two-dimensional and three-dimensional images. In recent pilot studies discussed in this paper, heavy-metal uptake by plant rootsin vivoand iron's phase distribution in the lithium–iron–phosphate cathode of a lithium-ion battery have been imaged. Also, the spatial resolution of computed tomography has been improved from 70 nm to 55 nm by means of run-out correction and application of a reconstruction algorithm.
Databáze: OpenAIRE
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