The effect of simulating body fluid on the structural properties of hydroxyapatite synthesized in the presence of citric acid
| Autor: | Omer Kaygili, Mustafa Kom, Sergey V. Dorozhkin, Serhat Keser, Niyazi Bulut |
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| Jazyk: | angličtina |
| Rok vydání: | 2016 |
| Předmět: |
Materials science
Scanning electron microscope Simulated body fluid 02 engineering and technology 010402 general chemistry 01 natural sciences Hydroxyapatite chemistry.chemical_compound Crystallinity Citric acid stomatognathic system Fourier transform infrared spectroscopy Spectroscopy Original Research Body fluid Bioceramics 021001 nanoscience & nanotechnology 0104 chemical sciences Crystallography chemistry General Earth and Planetary Sciences Crystallite 0210 nano-technology Nuclear chemistry |
| Zdroj: | Progress in Biomaterials |
| ISSN: | 2194-0517 2194-0509 |
| Popis: | In present work, the effect of citric acid (CA) addition in different amounts (0, 1, 5 and 10 ml) on the structure of hydroxyapatite (HAp) was investigated using X-ray diffraction (XRD), Fourier transform infrared (FTIR) spectroscopy, scanning electron microscopy (SEM) and energy dispersive X-ray (EDX) spectroscopy techniques. The crystallite dimensions, lattice parameters, unit cell volume, crystallinity percentage and Ca/P molar ratio were found to be affected by the CA content. To investigate the influence of CA on the bioactive properties of the HAp samples and to determine the optimum amount of CA, in vitro soaking tests in simulated body fluid (SBF) were performed. Although the samples' morphology was found to be affected by neither the amount of CA nor the soaking time in SBF, the soaking results revealed that the maximum changes in the Ca/P ratio were found for the HAp samples prepared in the presence of the highest amounts of CA, which pointed out to the highest bioactivity of these samples. |
| Databáze: | OpenAIRE |
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