Direct structure elucidation by powder X-ray diffraction of a metal-organic framework material prepared by solvent-free grinding
| Autor: | Fujii, Kotaro, Garay, A. L., Hill, J., Sbircea, E., Pan, Z. G., Xu, M. C., Apperley, D. C., James, S. L., Harris, K. D. M. |
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| Jazyk: | angličtina |
| Rok vydání: | 2010 |
| Předmět: |
Diffraction
Materials science Solvent free Metals and Alloys General Chemistry Powder xrd Catalysis Surfaces Coatings and Films Electronic Optical and Magnetic Materials Grinding Crystallography Microcrystalline Chemical engineering X-ray crystallography Materials Chemistry Ceramics and Composites Porosity |
| Zdroj: | Chemical Communications. 46:7572-7574 |
| ISSN: | 1359-7345 |
| Popis: | Powder X-ray diffraction (XRD) has been exploited to establish the structural properties of a porous interpenetrated mixed-ligand metal–organic framework material prepared by solid-state grinding, recognizing that product phases from mechanochemical synthesis are typically microcrystalline powders. The importance of subjecting the powder XRD data to rigorous scrutiny in such applications is emphasized. |
| Databáze: | OpenAIRE |
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