Ultrasound Assisted the Synthesis of 1,3-Dioxolane Derivatives from the Reaction of Epoxides or 1,2-Diols with Various Ketones Using Graphene Oxide Catalyst
Autor: | Rabah Boukherroub, Zahra Ahmadi, Maryam Mirza-Aghayan, Marzieh Mohammadi |
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Přispěvatelé: | Institut d’Électronique, de Microélectronique et de Nanotechnologie - UMR 8520 (IEMN), Centrale Lille-Institut supérieur de l'électronique et du numérique (ISEN)-Université de Valenciennes et du Hainaut-Cambrésis (UVHC)-Université de Lille-Centre National de la Recherche Scientifique (CNRS)-Université Polytechnique Hauts-de-France (UPHF), NanoBioInterfaces - IEMN (NBI - IEMN), Centrale Lille-Institut supérieur de l'électronique et du numérique (ISEN)-Université de Valenciennes et du Hainaut-Cambrésis (UVHC)-Université de Lille-Centre National de la Recherche Scientifique (CNRS)-Université Polytechnique Hauts-de-France (UPHF)-Centrale Lille-Institut supérieur de l'électronique et du numérique (ISEN)-Université de Valenciennes et du Hainaut-Cambrésis (UVHC)-Université de Lille-Centre National de la Recherche Scientifique (CNRS)-Université Polytechnique Hauts-de-France (UPHF) |
Rok vydání: | 2020 |
Předmět: |
Reaction conditions
010405 organic chemistry Graphene Oxide [CHIM.CATA]Chemical Sciences/Catalysis General Chemistry 010402 general chemistry Ultrasound assisted 01 natural sciences Combinatorial chemistry Catalysis 0104 chemical sciences law.invention chemistry.chemical_compound chemistry law Dioxolane ComputingMilieux_MISCELLANEOUS Organometallic chemistry Reusability |
Zdroj: | Catalysis Letters Catalysis Letters, Springer Verlag, 2020, 150 (10), pp.2959-2969. ⟨10.1007/s10562-020-03196-x⟩ Catalysis Letters, 2020, 150 (10), pp.2959-2969. ⟨10.1007/s10562-020-03196-x⟩ |
ISSN: | 1572-879X 1011-372X |
DOI: | 10.1007/s10562-020-03196-x |
Popis: | The main objective of this study concerns the sonochemical synthesis of 1,3-dioxolane derivatives using graphene oxide catalyst by applying two methods. In the first method, we described the synthesis of 1,3-dioxolane by ring-opening of epoxides in the presence of ketones catalyzed by graphene oxide (GO) under ultrasonic irradiation. In the second sonochemical procedure, we described the synthesis of 1,3-dioxolane derivatives by the reaction of 1,2-diols with ketones using same GO catalyst. Mild reaction conditions, high yields, short reaction times, reusability of catalyst and easy isolation of the products make the developed methods very useful. |
Databáze: | OpenAIRE |
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