A fast and low-cost dynamic calorimetric method for phase diagram estimation of binary systems
| Autor: | Clément Mailhé, M. Duquesne |
|---|---|
| Přispěvatelé: | Institut de Mécanique et d'Ingénierie (I2M), Université de Bordeaux (UB)-Institut Polytechnique de Bordeaux-Centre National de la Recherche Scientifique (CNRS)-Institut National de Recherche pour l’Agriculture, l’Alimentation et l’Environnement (INRAE)-Arts et Métiers Sciences et Technologies, HESAM Université (HESAM)-HESAM Université (HESAM) |
| Jazyk: | angličtina |
| Rok vydání: | 2020 |
| Předmět: |
Phase transition
Materials science Binary number Microbolometer 02 engineering and technology Calorimetry 021001 nanoscience & nanotechnology Condensed Matter Physics 01 natural sciences 010406 physical chemistry 0104 chemical sciences Phase diagram [SPI]Engineering Sciences [physics] Differential scanning calorimetry Phase transitions Fatty organic materials Thermography Infrared thermography Screening Physical and Theoretical Chemistry 0210 nano-technology Biological system Reliability (statistics) |
| Zdroj: | Journal of Thermal Analysis and Calorimetry Journal of Thermal Analysis and Calorimetry, Springer Verlag, 2020, pp.587-598. ⟨10.1007/s10973-020-09287-6⟩ |
| ISSN: | 1388-6150 1588-2926 |
| DOI: | 10.1007/s10973-020-09287-6⟩ |
| Popis: | A dynamic calorimetric method based on infrared thermography has been used for the phase diagram estimation of binary systems of fatty organic materials. Its promising results make of this innovative method an interesting asset in applications with time constraints. In order to provide a calorimetry method with satisfactory performance and the lowest time consumption and cost, a test campaign is undergoing. This campaign aims at evaluating the influence of operating conditions on the performances of the method. In that frame, the phase diagrams estimated using a high-end photon detector and a low-cost microbolometer are compared. The assessment of the accuracy and reliability of phase transitions detection is made based on the study of 4 binary systems of fatty acids and fatty alcohols. Differential scanning calorimetry is used for the validation of the experimental phase diagram, and further works are identified in the light of innovative data obtained using the infrared thermography method. |
| Databáze: | OpenAIRE |
| Externí odkaz: |
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