Design, Calibration and Testing of a New Macro-Thermogravimetric Analyzer
| Autor: | Quentin Balme, J. Sedan, Frederic Marias, F. Lemont, F. Rousset, P. Charvin, J. Bondroit |
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| Přispěvatelé: | Centre d'Energétique et de Thermique de Lyon (CETHIL), Université Claude Bernard Lyon 1 (UCBL), Université de Lyon-Université de Lyon-Institut National des Sciences Appliquées de Lyon (INSA Lyon), Université de Lyon-Institut National des Sciences Appliquées (INSA)-Institut National des Sciences Appliquées (INSA)-Centre National de la Recherche Scientifique (CNRS), Commissariat à l'énergie atomique et aux énergies alternatives (CEA), Laboratoire de Génie Thermique Énergétique et Procédés (EA1932) (LATEP), Université de Pau et des Pays de l'Adour (UPPA), Centre National de la Recherche Scientifique (CNRS)-Institut National des Sciences Appliquées de Lyon (INSA Lyon), Université de Lyon-Institut National des Sciences Appliquées (INSA)-Université de Lyon-Institut National des Sciences Appliquées (INSA)-Université Claude Bernard Lyon 1 (UCBL), Université de Lyon, LABORATOIRE DE THERMIQUE ENERGETIQUE ET PROCEDES (EA1932) (LATEP) |
| Jazyk: | angličtina |
| Rok vydání: | 2018 |
| Předmět: |
Thermogravimetric analysis
Spectrum analyzer Materials science 020209 energy education Analytical chemistry 02 engineering and technology Polyethylene Condensed Matter Physics Combustion musculoskeletal system scopusₗatep chemistry.chemical_compound surgical procedures operative 020401 chemical engineering chemistry 0202 electrical engineering electronic engineering information engineering Calibration [SPI.GPROC]Engineering Sciences [physics]/Chemical and Process Engineering 0204 chemical engineering Physical and Theoretical Chemistry Macro human activities health care economics and organizations |
| Zdroj: | Journal of Thermal Analysis and Calorimetry Journal of Thermal Analysis and Calorimetry, 2018, 132 (3), pp.1439-1447. ⟨10.1007/s10973-018-7118-x⟩ Journal of Thermal Analysis and Calorimetry, Springer Verlag, 2018, 132 (3), pp.1439-1447. ⟨10.1007/s10973-018-7118-x⟩ |
| ISSN: | 1388-6150 1588-2926 |
| DOI: | 10.1007/s10973-018-7118-x⟩ |
| Popis: | The design and development of a macro-thermogravimetric (TG) analyzer are presented. Two sources of measurement bias are studied: balance heating and the effect of viscous forces. Temperature regulation and measurement are discussed. In a second part of the study, results obtained with the newly developed macro-TG system for the dehydration of CuSO4·5H2O are compared with data obtained with a commercial thermobalance. The effects of mass and of the heating rate on TG and differential TG curves are discussed. Finally, the effect of the initial mass of a polyethylene sample on its combustion is studied as an example application of the macro-TG device. |
| Databáze: | OpenAIRE |
| Externí odkaz: |
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