Identifying method validation and measurement uncertainty of brominated vegetable oil in soft drinks and carbonated waters commonly consumed in South Korea
| Autor: | Tae-Dong Jung, Gunyoung Lee, Jin-Ha Lee, Bong-Yeon Cho, Ok-Hwan Lee, Seong-Ran Kang, Seung-Hyun Choi, Sang Soon Yun, Ho Soo Lim, Sun-Il Choi, Jae-Min Kim |
|---|---|
| Rok vydání: | 2018 |
| Předmět: |
Quality Control
Food Safety food.ingredient Halogenation Ion chromatography Carbonated Beverages Mass spectrometry 01 natural sciences Gas Chromatography-Mass Spectrometry Analytical Chemistry Brominated vegetable oil 0404 agricultural biotechnology food Republic of Korea Humans Plant Oils Food science Fatty Acids 010401 analytical chemistry Uncertainty Reproducibility of Results 04 agricultural and veterinary sciences General Medicine 040401 food science 0104 chemical sciences Carbonated Water Measurement uncertainty Environmental science Gas chromatography Gas chromatography–mass spectrometry Food Science |
| Zdroj: | Food Chemistry. 246:323-327 |
| ISSN: | 0308-8146 |
| DOI: | 10.1016/j.foodchem.2017.11.047 |
| Popis: | This study investigated a method for validating and determining the measurement uncertainty for the composition of brominated vegetable oil (BVO) in soft drinks and carbonated waters commonly consumed in South Korea. First, we studied a simple and precise qualitative colorimetric method at the maximum residues level 15 ppm. And an analytical method using ion chromatography (IC) was validated and identified with brominated fatty acids by gas chromatography electron ionization mass spectrometry (GC/EI-MS). The measurement uncertainty was evaluated based on the precisional study and confirmed by the preliminary inter-laboratory study. For IC analysis, the recovery range of BVO was from 97.8% to 107.2% with relative standard deviations between 0.18% and 0.69%. In addition, the expanded uncertainty of the BVO was 1.59. These results indicate that the validated method is appropriate for identifying of BVO and can be used to verify the safety of soft drinks or carbonated waters containing BVO residues. |
| Databáze: | OpenAIRE |
| Externí odkaz: |
|
Full Text from ScienceDirect