Electrolytic dissolution for constituents determination in tool steels by ICP-AES

Autor:	Boaventura F. Reis, Henrique Bergamin Filho, Ana Paula G. Gervasio, Maria Fernanda Georgina Giné-Rosias
Jazyk:	portugalština
Rok vydání:	2000
Předmět:	Analyte Materials science emission spectrometry Analytical chemistry electrolytic dissolution General Chemistry Metal analysis lcsh:Chemistry Chemistry Acid dissolution lcsh:QD1-999 flow system tool steels QD1-999 Dissolution
Zdroj:	Química Nova v.23 n.4 2000 Química Nova Sociedade Brasileira de Química (SBQ) instacron:SBQ Química Nova, Volume: 23, Issue: 4, Pages: 482-486, Published: AUG 2000 Química Nova, Vol 23, Iss 4, Pp 482-486 (2000)
Popis:	Different methods have been applied to solve special problems of metal analysis. First, the solid samples of tool steels were analyzed by X-ray fluorescence. Alternatively, an on-line electrodissolution implemented in a flow injection system and conventional dissolution procedure for determination of W, Mo, V and Cr in tool steels by ICP-AES is described. The resulting analyte solutions were compared with conventional dissolution procedure and determination by ICP-AES. The electrolytic procedure presented a good performance characterized by a sample throughput of 164 determinations per hour. Results were in agreement with those obtained by conventional acid dissolution.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_dedup___::ae743928c59b49413e9a7f8dd888f2bf http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0100-40422000000400010 Zobrazit plný text záznamu