Determination of optimization parameters based on the Box-Behnken design for cloud point extraction of quinoline yellow using Brij 58 and application of this method to real samples
| Autor: | Tufan Güray, Begüm Menevşe, Arzu Altin Yavuz |
|---|---|
| Rok vydání: | 2020 |
| Předmět: |
food.ingredient
Octoxynol Ether 02 engineering and technology Polyethylene glycol 010402 general chemistry 01 natural sciences Analytical Chemistry Polyethylene Glycols chemistry.chemical_compound Surface-Active Agents food Instrumentation Spectroscopy Detection limit Cloud point Chromatography Food additive Quinoline Extraction (chemistry) Hydrogen-Ion Concentration 021001 nanoscience & nanotechnology Box–Behnken design Atomic and Molecular Physics and Optics 0104 chemical sciences chemistry Spectrophotometry Quinolines Cetomacrogol 0210 nano-technology |
| Zdroj: | Spectrochimica acta. Part A, Molecular and biomolecular spectroscopy. 243 |
| ISSN: | 1873-3557 |
| Popis: | Quinoline yellow (E104) dye is a food additive and generally used in cosmetics and drugs. In this work, polyethylene glycol hexa decyl ether (Brij 58) was used for the spectrophotometric determination of quinoline yellow (QY) in food and drug samples after cloud point extraction (CPE). Some parameters such as extraction temperature and time, pH, centrifuge speed, Brij 58 (surfactant) concentration, and Na2SO4 concentration were optimized using Box-Behnken design. The limit of detection (LOD) of this method was 0.0019 μg mL−1 for QY while the relative standard deviation (RSD) at low concentration levels (0.03 μg mL−1) was 1.32% (n = 5). Findings indicated that, this novel CPE method can be used quickly for the reproducible, selective and sensitive determination of QY dye in ordinary analysis. |
| Databáze: | OpenAIRE |
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