Simplified preparation of 16-dehydropregnenolone acetate
| Autor: | Milovan D. Ivanović, David M. Piatak, Ivan V. Mićović |
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| Rok vydání: | 1990 |
| Předmět: |
Chromatography
010405 organic chemistry Organic Chemistry Industrial scale Diosgenin 010402 general chemistry 01 natural sciences Catalysis 0104 chemical sciences Pressure range Dehydropregnenolone acetate chemistry.chemical_compound Reduced properties chemistry Yield (chemistry) One pot reaction Organic chemistry |
| Zdroj: | Synthesis, Stuttgart |
| Popis: | A simplified, one-pot preparation of 16-dehydropregnenolone acetate from diosgenin using normal pressure and a much reduced temperature compared to known procedure was developed in an overall yield varied from 65 to 69 %. The method lends itself very well to industrial scale methodology |
| Databáze: | OpenAIRE |
| Externí odkaz: |
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