[Validation Study on a Multi-Residue Method for Determination of Pesticide Residues in Vegetables and Fruits by using General Matrix Standard Solutions]
| Autor: | Satoshi Takatori, Satoko Yamaguchi, Hirotaka Obana, Masato Yoshimitsu, Masakazu Osakada, Naoki Fukui, Keiji Kajimura, Yoko Kitagawa |
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| Rok vydání: | 2015 |
| Předmět: |
Multi residue
Validation study Chromatography Chromatography Gas Pesticide residue Pesticide Residues Food Contamination General Medicine Standard solution Pesticide Organophosphates Polyethylene Glycols Solutions Tandem Mass Spectrometry Fruit Vegetables Food science Gas chromatography General matrix Food Analysis Mathematics |
| Zdroj: | Shokuhin eiseigaku zasshi. Journal of the Food Hygienic Society of Japan. 56(4) |
| ISSN: | 1882-1006 |
| Popis: | Quantitative methods using the matrix-matched standard solutions approach are widely used for multi-residue pesticide determination by GC-MS/MS to deal with the issue of matrix effects. However, preparing matrix-matched standard solutions in analyses of many kinds of samples is very time-consuming. In order to solve this problem, a method that employs general matrix standard solutions has been developed using polyethylene glycol (PEG), extract of vegetables-fruit juice (VFJm) and triphenyl phosphate (named the PEG-VFJm method). Here, a validation study for 168 pesticides was performed on three kinds of samples [potato, spinach and apple] at concentrations of 0.010 and 0.050 μg/g. In these three commodities, 144 to 158 pesticides satisfied the required criteria using the matrix-matched method and 129 to 149 pesticides satisfied the same criteria using the PEG-VFJm method. Our results suggest that application of general matrix standard solutions would enable rapid and effective analyses of pesticides. |
| Databáze: | OpenAIRE |
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