Imaging columns of the light elements carbon, nitrogen and oxygen with sub Angstrom resolution

Autor: Michael A. O'Keefe, Andreas Thust, C. J. D. Hetherington, R. Kilaas, Yang Wang, Christian Kisielowski
Jazyk: angličtina
Rok vydání: 2016
Předmět:
Popis: It is reported that lattice imaging with a 300 kV field emission microscope in combination with numerical reconstruction procedures can be used to reach an interpretable resolution of about 80 pm for the first time. A retrieval of the electron exit wave from focal series allows for the resolution of single atomic columns of the light elements carbon, nitrogen, and oxygen at a projected nearest neighbor spacing down to 85 pm. Lens aberrations are corrected on-line during the experiment and by hardware such that resulting image distortions are below 80 pm. Consequently, the imaging can be aberration-free to this extent. The resolution enhancement results from increased electrical and mechanical stability's of the instrument coupled with a low spherical aberration coefficient of 0.595 + 0.005 mm.
Databáze: OpenAIRE