Evolution of stress fields during crack growth and arrest in a brittle-ductile CrN-Cr clamped-cantilever analysed by X-ray nanodiffraction and modelling
Autor: | Alexander M. Korsunsky, Martin Rosenthal, Rostislav Daniel, Hynek Hruby, Jozef Keckes, Jakub Zalesak, Michael Meindlhumer, León Romano Brandt, Enrico Salvati, Christian Mitterer, Jaromír Kopeček, Juraj Todt |
---|---|
Rok vydání: | 2021 |
Předmět: |
Technology
STRAIN Materials science Cantilever Materials Science Cross-sectional X-ray nanodiffraction GRADIENTS Materials Science Multidisciplinary TEXTURE 02 engineering and technology Cr CrN Eigenstrain modelling Micromechanics Multi-layer RESIDUAL-STRESS MICROSCALE 010402 general chemistry FATIGUE 01 natural sciences FRACTURE-TOUGHNESS Stress (mechanics) THIN-FILMS Fracture toughness Brittleness Eigensrrain modelling Residual stress lcsh:TA401-492 General Materials Science Composite material Stress intensity factor COATINGS Science & Technology Mechanical Engineering 021001 nanoscience & nanotechnology 0104 chemical sciences Mechanics of Materials Fracture (geology) lcsh:Materials of engineering and construction. Mechanics of materials MICROSTRUCTURE Deformation (engineering) 0210 nano-technology |
Zdroj: | Materials & Design, Vol 198, Iss, Pp 109365-(2021) 'Materials and Design ', vol: 198, pages: 109365-1-109365-16 (2021) |
ISSN: | 0264-1275 0261-3069 |
Popis: | In order to understand the fracture resistance of nanocrystalline thin films, it is necessary to assess nanoscopic multiaxial stress fields accompanying crack growth during irreversible deformation. Here, a clamped cantilever with dimensions of 200×23.7×40μm3was machined by focused ion beam milling from a thin film composed of four alternating CrN and Cr layers. The cantilever was loaded to 460 mN in two steps and multiaxial strain distributions were determined byin situcross-sectional X-ray nanodiffraction. Characterization in as-deposited state revealed the depth variation of fibre texture and residual stress across the layers. Thein situexperiment indicated a strong influence of the residual stresses on the cross-sectional stress fields evolution and crack arrest capability at the CrN-Cr interface. In detail, an effective negative stress intensity of −5.9±0.4MPam½arose as a consequence of the residual stress state. Crack growth in the notched Cr layer occurred at a critical stress intensity of 2.8±0.5MPam½. The results were complemented by two-dimensional numerical simulation to gain further insight into the elastic-plastic deformation evolution. The quantitative experimental and modelling results elucidate the stepwise nature of fracture advancement across the alternating brittle and ductile layers and their interfaces. |
Databáze: | OpenAIRE |
Externí odkaz: |