A structural investigation of tris(ethyl acetoacetate)aluminium (III)
| Autor: | Emilija Tkalčec, Ivan Simčić, Xavier Rocquefelte, A. G. G. Moliterni, T. Gazivoda Kraljević, Angela Altomare, Stanislav Kurajica, Vilko Mandić, Jasminka Popović |
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| Rok vydání: | 2014 |
| Předmět: |
Tris
Materials science Structure determination form XRPD Scanning electron microscope Inorganic chemistry chemistry.chemical_element General Chemistry Crystal structure Nuclear magnetic resonance spectroscopy Condensed Matter Physics Electronic Optical and Magnetic Materials Biomaterials chemistry.chemical_compound Crystallography NMR spectroscopy Tris(ethyl acetoacetate) aluminium (III) chemistry Aluminium Ethyl acetoacetate Materials Chemistry Ceramics and Composites structure determination form XRPD tris(ethyl acetoacetate) aluminium (III) Powder diffraction Monoclinic crystal system |
| Zdroj: | Journal of sol-gel science and technology 71 (2014): 217–223. doi:10.1007/s10971-014-3345-1 info:cnr-pdr/source/autori:Kurajica, S.; Popovic, J.; Kraljevic, T. G.; Tkalcec, E.; Simcic, I.; Mandic, V.; Altomare, A.; Moliterni, A.; Rocquefelte, X./titolo:A structural investigation of tris(ethyl acetoacetate)aluminium (III)/doi:10.1007%2Fs10971-014-3345-1/rivista:Journal of sol-gel science and technology/anno:2014/pagina_da:217/pagina_a:223/intervallo_pagine:217–223/volume:71 |
| ISSN: | 1573-4846 0928-0707 |
| DOI: | 10.1007/s10971-014-3345-1 |
| Popis: | Aluminium tris(ethyl acetoacetate), Al(C6H9O3)(3) has been prepared and characterized by means of H-1 and C-13 nuclear magnetic resonance spectroscopy, scanning electron microscopy and X-ray powder diffraction (XRPD). It was determined that two stereoisomeric complexes can be distinguished in the solution: meridional and facial. The crystal structure of Al(C6H9O3)(3) has been determined from XRPD data. The compound crystallizes in the monoclinic space group P2(1)/n. |
| Databáze: | OpenAIRE |
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