Controlling the electrodeposition, morphology and structure of hydroxyapatite coating on 316L stainless steel
| Autor: | Dinh Thi Mai Thanh, Tran Dai Lam, Pham Thi Nam, Nguyen Van Anh, Nguyen Thu Phuong, Thai Hoang, Le Xuan Que |
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| Rok vydání: | 2012 |
| Předmět: |
Materials science
Time Factors Scanning electron microscope Bioengineering Electrolyte engineering.material Biomaterials Electrolytes Coating Coated Materials Biocompatible Electricity X-Ray Diffraction Microscopy Spectroscopy Fourier Transform Infrared Fourier transform infrared spectroscopy Polarization (electrochemistry) Electrodes Metallurgy Temperature Spectrometry X-Ray Emission Hydrogen Peroxide Stainless Steel Electroplating Molecular Weight Solutions Durapatite Chemical engineering Mechanics of Materials Electrode X-ray crystallography engineering Microscopy Electron Scanning |
| Zdroj: | Materials scienceengineering. C, Materials for biological applications. 33(4) |
| ISSN: | 1873-0191 |
| Popis: | Hydroxyapatite (HAp) coatings were prepared on 316L stainless steel (316LSS) substrates by electrochemical deposition in the solutions containing Ca(NO3)2·4H2O and NH4H2PO4 at different electrolyte concentrations. Along with the effect of precursor concentration, the influence of temperature and H2O2 content on the morphology, structure and composition of the coating was thoroughly discussed with the help of X-ray diffraction (XRD), Scanning electron microscopy (SEM), Fourier transform infrared (FTIR) spectra. The in vitro tests in simulated body fluids (SBF) were carried out and then the morphological and structural changes were estimated by SEM and electrochemical techniques (open circuit potential, polarization curves, Nyquist and Bode spectra measurements). Being simple and cost-effective, this method is advantageous for producing HAp implant materials with good properties/characteristics, aiming towards in vivo biomedical applications. |
| Databáze: | OpenAIRE |
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