Synthesis, growth and characterization of organic crystal triphenylmethane p-nitroaniline: a nonlinear optical crystal
| Autor: | G. Bhuvaneswari, L. Guru Prasad, N. Prabhavathi |
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| Jazyk: | angličtina |
| Rok vydání: | 2017 |
| Předmět: |
Materials science
uv-vis spectroscopy nonlinear optical material Crystal growth 010402 general chemistry Photochemistry 01 natural sciences Nanomaterials dielectric studies 010309 optics chemistry.chemical_compound Ultraviolet visible spectroscopy 0103 physical sciences General Materials Science Fourier transform infrared spectroscopy Materials of engineering and construction. Mechanics of materials ft-ir Triphenylmethane xrd Mechanical Engineering P-Nitroaniline crystal growth Organic crystal Condensed Matter Physics 0104 chemical sciences Characterization (materials science) chemistry Mechanics of Materials TA401-492 |
| Zdroj: | Materials Science-Poland, Vol 35, Iss 3, Pp 667-672 (2017) |
| Popis: | A triphenylmethane-4-nitroaniline salt has been synthesized and the crystals have been grown by using slow evaporation solution growth technique. The grown single crystal was investigated by recording the powder XRD, FT-IR spectrum, UV-Vis spectrum, Vickers microhardness test, dielectric measurements and powder SHG. The growth of crystal was confirmed by analyzing the XRD pattern and it was stated that the grown material crystallized in triclinic system. Vibrational peaks of the functional groups existing in the compound were identified. Vickers microhardness studies were carried to measure the mechanical strength. In order to identify the phase transition temperature, the dielectric studies were carried out at different temperatures. Dielectric constant, dielectric loss and impedance of the crystal were monitored with respect to the frequency of electric field. |
| Databáze: | OpenAIRE |
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