Influence of extrusion conditions on fiber breakage along the screw profile during twin screw compounding of glass fiber-reinforced PA

Autor: Rudy Valette, Nessim Ghamri, Bruno Vergnes, Jean-Laurent Pradel, Julien Ville, Audrey Durin, Funda Inceoglu
Přispěvatelé: Laboratoire d'Ingénierie des Matériaux de Bretagne (LIMATB), Université de Bretagne Sud (UBS)-Institut Brestois du Numérique et des Mathématiques (IBNM), Université de Brest (UBO)-Université de Brest (UBO)-Université de Brest (UBO), Centre de recherche, développement, applications et technique de l'ouest (CERDATO), Arkema (Arkema), Centre de Mise en Forme des Matériaux (CEMEF), MINES ParisTech - École nationale supérieure des mines de Paris, Université Paris sciences et lettres (PSL)-Université Paris sciences et lettres (PSL)-Centre National de la Recherche Scientifique (CNRS)
Jazyk: angličtina
Rok vydání: 2013
Předmět:
Zdroj: International Polymer Processing
International Polymer Processing, 2013, 28 (1), pp.49-57. ⟨10.3139/217.2659⟩
Popis: In the present study, Polyamide 12 was compounded with glass fibers in both laboratory and industrial twin screw extruders using various processing conditions (screw speed and feed rate). Dead-stop experiments were performed and samples were collected at different locations along the screws in order to determine the fiber length distribution and the extent of fiber breakage. Results show that significant fiber break-up occurs right after the addition of glass fibers to the molten matrix. Similarly fiber length distribution changes drastically at the first sampling location, near the glass fiber feeder. Processing conditions also influence the extent of degradation: it increases with screw speed and decreases with feed rate, which controls the residence time. Flow modelling has been used to calculate the flow conditions along the screw profile. It is shown that the modified Shon-Liu-White model previously proposed to describe the average fiber length evolution as function of specific energy is not able to correctly predict the evolution along the screw profile. In similar processing conditions, the large industrial extruder appears as less severe than the small laboratory one.
Databáze: OpenAIRE