Microstructure and mechanical properties of borided CoCrFeNiAl0.25Ti0.5 high entropy alloy produced by powder metallurgy

Autor: Sakin Zeytin, Mustafa Sabri Gök, Ali Günen, Azmi Erdogan
Přispěvatelé: Mühendislik ve Doğa Bilimleri Fakültesi -- Metalurji ve Malzeme Mühendisliği Bölümü, Günen, Ali
Rok vydání: 2021
Předmět:
Sintered samples
Fracture-toughness
Powder metals
Fracture toughness values
Powder mixtures
Cobalt alloys
Entropy
Chromium metallurgy
Mechanical properties
Borides
Chromium Borides
chemistry.chemical_compound
Complex metals
Fracture toughness
Relative density
Powder metallurgy
Densification
Iron alloys
Ti
Instrumentation
Iron metallurgy
Microstructure
Work tool steel
Multidisciplinary
Surface hardness
Nickel metallurgy
Condensed Matter Physics
Hardness
Surfaces
Coatings and Films

High entropy alloy
Silicides
Materials science
High-entropy alloys
Iron
Materials Science
Diffusion kinetics
Physics
Applied

Surface roughness
Boride
Titanium alloys
Boron carbide
Cobalt metallurgy
Powder mixture
Boriding
Sodium compounds
Behavior
Titanium metallurgy
CoCrFeNiAl0.25Ti0.5
Metallurgy
Chromium alloys
Nanoindentation
Boriding process
Microstructure and mechanical properties
Aluminum alloys
chemistry
Aluminum metallurgy
Nimonic Alloys
Zdroj: VACUUM
Popis: CoCrFeNiAl0.25Ti0.5 high entropy alloy alloys (HEA), produced by powder metallurgy were subjected to boriding to improve their mechanical properties. Sintering was carried out at 1200 degrees C for 2 h in Ar, and boriding was performed at 900, 1000 and 1100 degrees C for 2 h using a 90 wt% B4C + 10 wt% NaBF4 boriding powder mixture. Microstructures, densities, surface roughnesses, and mechanical properties (hardness, fracture toughness and nanoindentation responses) of the samples were investigated. FCC, BCC and sigma phases had been observed after sintering, whereas complex metal borides were formed on the surfaces after boriding. Relative density values were between 85% and 90%. Significant increases in surface hardness were observed after boriding due to formation of hard, silicide-free boride layers. The boride layer thickness and hardness increased with increasing boriding temperature. The elastic modulus of the surface of the sintered sample (47.07 GPa) increased with the boriding process to values in the range of 140-151 GPa. Fracture toughness values between 3.57 and 4.25 MPa m(1/2) were obtained in borided samples, and increasing the boriding temperature reduced the fracture toughness.
Databáze: OpenAIRE