1-nitroso-2-naphthol impregnated multiwalled carbon nanotubes (NNMWCNTs) for the separation-enrichment and flame atomic absorption spectrometric detection of copper and lead in hair, water, and food samples
| Autor: | Mohamed A. Habila, Erkan Yilmaz, Zeid A. ALOthman, Mustafa Soylak |
|---|---|
| Rok vydání: | 2017 |
| Předmět: |
Chemistry
Inorganic chemistry Analytical chemistry chemistry.chemical_element 02 engineering and technology 1 nitroso 2 naphthol 010402 general chemistry 021001 nanoscience & nanotechnology Multiwalled carbon 01 natural sciences Copper 0104 chemical sciences law.invention law 0210 nano-technology Atomic absorption spectroscopy |
| Zdroj: | DESALINATION AND WATER TREATMENT. 87:285-291 |
| DOI: | 10.5004/dwt.2017.21296 |
| Popis: | A novel enrichment-separation procedure based on solid phase extraction of copper(II) and lead(II) at ultratrace levels on 1-nitroso-2-naphthol impregnated multiwalled carbon nanotubes (NNMWCNTs) has been established. The effective critical parameters like pH and eluent type etc. on the quantitative recoveries of the analyte elements were optimized. The matrix effects are also investigated. The procedure was validated by analysing water certified reference materials and addition-recovery tests. The relative standard deviation of the presented procedure was below 10%. The application of the presented solid phase extraction procedure was successfully performed for copper and lead determination in some food and water samples. |
| Databáze: | OpenAIRE |
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