Determination and Confirmation of Parent and Total Ractopamine in Bovine, Swine, and Turkey Tissues by Liquid Chromatography with Tandem Mass Spectrometry: Final Action 2011.23
| Autor: | Mark R Coleman, Sharon L Brunelle, Thomas J Burnett, Kimberly R Lombardi, W Dennis Ulrey |
|---|---|
| Rok vydání: | 2013 |
| Předmět: |
Liver chemistry
Turkeys Swine Tandem mass spectrometry Analytical Chemistry chemistry.chemical_compound Tandem Mass Spectrometry Phenethylamines Animals Environmental Chemistry Medicine Bovine muscle Growth Substances Pharmacology Chromatography business.industry Muscles Drug Residues Ractopamine Liver chemistry Invalid Data Cattle Action status business Agronomy and Crop Science Chromatography Liquid Food Science |
| Zdroj: | Journal of AOAC INTERNATIONAL. 96:917-924 |
| ISSN: | 1944-7922 1060-3271 |
| DOI: | 10.5740/jaoacint.12-395 |
| Popis: | A multilaboratory study of AOAC Official MethodSM 2011.23 was performed to satisfy requirements for Final Action status through the AOAC expert review panel process. The study included nine collaborating laboratories from the United States, Canada, Brazil, and The Netherlands. Five incurred residue materials (bovine muscle, bovine liver, swine muscle, swine liver, and turkey muscle) were analyzed by each laboratory as blind duplicates for parent and total ractopamine content. After removal of invalid data, the parent and total ractopamine methods demonstrated acceptable reproducibility (RSDR 11.4–42.4%, HorRatR 0.34–2.01) based on AOAC criteria. The method was awarded Final Action status by the Official Methods Board on October 4, 2012. |
| Databáze: | OpenAIRE |
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