Step-by-step synthesis of iron-oxide nanoparticles attached to graphene oxide: A study on the composite properties and architecture
Autor: | Marcelo Knobel, Patricia C. Rivas Rojas, Leandro M. Socolovsky, Oscar Moscoso Londoño, Pablo Tancredi |
---|---|
Jazyk: | angličtina |
Rok vydání: | 2018 |
Předmět: |
Materials science
Composite number Oxide 02 engineering and technology INGENIERÍAS Y TECNOLOGÍAS 010402 general chemistry 01 natural sciences law.invention chemistry.chemical_compound law General Materials Science Nanotecnología Nanocomposite Graphene GRAPHENE-OXIDE Mechanical Engineering SAXS 021001 nanoscience & nanotechnology Condensed Matter Physics Nano-materiales NANOCOMPOSITES 0104 chemical sciences chemistry Chemical engineering MAGNETIC-NANOPARTICLES Mechanics of Materials MAGNETOMETRY Magnetic nanoparticles 0210 nano-technology Iron oxide nanoparticles |
Popis: | A set of nanocomposites made of iron oxide nanoparticles covalently bonded to graphene oxide and reduced graphene oxide was successfully prepared. The synthesis was carried out in a precise step-by-step process in order to carefully control the nanocomposite formation. The nanocomposites were characterized by a range of techniques to verify the components arrangement according to the proposed strategy. Over the different samples, an in-depth study by Small Angle X-Ray Scattering (SAXS) and DC-Magnetometry was accomplished to analyze in detail the structure and properties of the systems. The results from this work indicate that the increase of the nanoparticle to graphene oxide ratio and the chemical reduction from graphene oxide to reduced graphene oxide modify the spatial distribution and the architecture of the nanoparticles over the sheets, leading to the formation of localized assemblies and bundle-like structures that have a significant impact on the macroscopicmagnetic behavior. Fil: Tancredi Gentili, Pablo. Consejo Nacional de Investigaciones Científicas y Técnicas. Oficina de Coordinación Administrativa Houssay. Instituto de Tecnologías y Ciencias de la Ingeniería "Hilario Fernández Long". Universidad de Buenos Aires. Facultad de Ingeniería. Instituto de Tecnologías y Ciencias de la Ingeniería "Hilario Fernández Long"; Argentina Fil: Moscoso Londoño, Oscar. Universidad Autónoma de Manizales; Colombia. Universidade Estadual de Campinas; Brasil Fil: Rivas Rojas, Patricia Carolina. Consejo Nacional de Investigaciones Científicas y Técnicas. Oficina de Coordinación Administrativa Houssay. Instituto de Tecnologías y Ciencias de la Ingeniería "Hilario Fernández Long". Universidad de Buenos Aires. Facultad de Ingeniería. Instituto de Tecnologías y Ciencias de la Ingeniería "Hilario Fernández Long"; Argentina Fil: Knobel, Marcelo. Universidade Estadual de Campinas; Brasil Fil: Socolovsky, Leandro Martín. Universidad Tecnológica Nacional; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas; Argentina |
Databáze: | OpenAIRE |
Externí odkaz: |