Examining slit pore widths within plasma-exfoliated graphitic material utilising Barret-Joyner-Halenda analysis
| Autor: | Christian J. Laycock, Rachel L. McLaren, Gareth R. Owen, Emmanuel Bruno Jean Paul Brousseau |
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| Jazyk: | angličtina |
| Rok vydání: | 2021 |
| Předmět: |
Diffraction
Chemistry Scanning electron microscope 02 engineering and technology General Chemistry 010402 general chemistry 021001 nanoscience & nanotechnology 01 natural sciences Catalysis 0104 chemical sciences symbols.namesake Chemical engineering X-ray photoelectron spectroscopy Stack (abstract data type) Transmission electron microscopy Materials Chemistry symbols 0210 nano-technology Porosity Dispersion (chemistry) Raman spectroscopy |
| ISSN: | 1144-0546 |
| Popis: | Plasma-exfoliated multilayer graphitic material (MLG) consists of orderly aligned stacks which contain many partially oxidised graphitic layers. Slit pores are present between successive stacks and their presence allows for improved friability, facile dispersion and accessibility for the intercalation of compounds. Whilst much research exists into the synthesis and application of MLG, there is a lack of quantitative data regarding their porous structures. This report outlines the structure of MLG as well as the application of Barrett–Joyner–Halenda (BJH) analysis to estimate the distance between adjacent stacks of orderly aligned graphitic layers within MLG. It was found that the distance between stacks can vary quite substantially between 2–131 nm within these plasma-derived materials, correlating with the width of meso- and macro-slit pores. Furthermore, t-plot data also suggests that micropores, likely to exist in the form of both slit pores and in-plane pores, are present within the material, hence stack separations may also exhibit distances of |
| Databáze: | OpenAIRE |
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