Preparation and chemical characterization of high purity fluorapatite

Autor:	I. Kotsis, P. Zimány, Pál Halmos, R. Fábián
Rok vydání:	1998
Předmět:	Reproducibility Chemistry Fluorapatite Analytical chemistry chemistry.chemical_element Apatite Analytical Chemistry Characterization (materials science) visual_art Argon gas Electrode visual_art.visual_art_medium Fluorine Titration
Zdroj:	Talanta. 46:1273-1277
ISSN:	0039-9140
DOI:	10.1016/s0039-9140(97)00391-3
Popis:	High purity fluorapatite (FAP) was prepared by solid state reaction, in flowing argon gas, at 1370 degrees C for 60 min. For chemical characterization of Ca(10)(PO(4))(6)F(2), the accuracy and reproducibility of different analytical methods were assessed. Methods with a good accuracy for the determination of Ca, P and F content were: titrations with EDTA for Ca determination (accuracy: -0.8%), spectrophotometric method for P determination (accuracy: +0.6%) and measurements with fluoride-selective electrode (accuracy +5.4%) for F determination.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_dedup___::85e258ba4e94b6fee5cb5eb6d9ee8480 https://doi.org/10.1016/s0039-9140(97)00391-3 Zobrazit plný text záznamu Full Text from ScienceDirect