The Oxford-Diamond In Situ Cell for studying chemical reactions using time-resolved X-ray diffraction

Autor:	Andrew Jupe, Saul J. Moorhouse, Nenad Vranješ, Michael Drakopoulos, Dermot O'Hare
Jazyk:	angličtina
Rok vydání:	2012
Předmět:	Diffraction In situ Materials science Beamline X-ray crystallography engineering Analytical chemistry Diamond Glassy carbon engineering.material Instrumentation Chemical reaction Hydrothermal circulation
Zdroj:	The Review of scientific instruments. 83(8)
ISSN:	1089-7623 0034-6748
Popis:	A versatile, infrared-heated, chemical reaction cell has been assembled and commissioned for the in situ study of a range of chemical syntheses using time-resolved energy-dispersive X-ray diffraction (EDXRD) on Beamline I12 at the Diamond Light Source. Specialized reactor configurations have been constructed to enable in situ EDXRD investigation of samples under non-ambient conditions. Chemical reactions can be studied using a range of sample vessels such as alumina crucibles, steel hydrothermal autoclaves, and glassy carbon tubes, at temperatures up to 1200 °C.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_dedup___::85a897e42008083def39ebd9b3ce4980 http://ora.ox.ac.uk/objects/uuid:2e927239-32dc-4ec0-80a8-a8c3cd67dfb9 Zobrazit plný text záznamu